Effect of water content on the flexural strength during refiring in dental porcelain / 대한치과보철학회지

STATEMENT OF PROBLEM: Long-term exposure of dental porcelain to saliva during temporary cementation of a porcelain-fused to metal (PFM) restoration could affect mechanical strength of dental porcelain if the restoration is refired. PURPOSE: This work was performed to verify the effect of water on the mechanical strength in aged dental porcelain. MATERIAL AND METHOD: 63 specimens(Vintage Metalbond opaque and opal powder) were distributed to three experimental groups; non-water immersed control, immersed and pedried, and immersed and non-predired groups. The changes in flexural strength and fracture toughness after specimen refiring related to Fourier Transform Infrared (FT-IR) spectroscopy. RESULTS: 1. The FT-IR reflectances assigned to molecular bonds of H2O were noted as significantly different between the first-fired group and three refired groups and between two water-immersed groups and control group after refiring( p<0.05). They were also significantly different between predried group and non-predried group after refiring( p<0.05). 2. For opal specimens, FT-IR absorbances for hydrogen bond of H2O and silanols were significantly higher in non-predried group than in predreid group( p<0.05). 3. Predried opal group showed the highest mean flexural strength( p<0.05). Non-predried group indicated higher mean flexural strength than control group( p<0.05). 4. The mean fracture toughness for predired group was higher than non-predried group( p<0.05). 5. The difference of leucite crystal size is noted between control group and water-immersed, predried group in scanning electron microscopic study(x10000).

COMPARISON OF SHEAR BOND STRENGTH AND MARGINAL LEAKAGE OF RESIN MODIFIED GLASS IONOMER CEMENTS / 대한치과보철학회지

The resin modified glass ionomer cements(RMGICs) have been used for years since 1989. Recently it has been developed for luting of fixed restorations. To evaluate the bond strength and marginal leakage of RMGICs for luting usage, the 80 extracted human molars which had uniform area of exposed dentin were cemented with 3 types of RMGICs(Fuji Duet, Advance, Vitremer), a conventional Glass Ionomer Cement(GIC-Fuji I), and a resin cement (Panavia 21) to base metal alloy(Ni-Cr-Be). After thermocycling the specimens were immersed in basic fuschin dye for measuring marginal leakage. The shear bond strength was measured with Instron and the maximum dye penetration was measured to 0.1mm. The type of fractured patterns were determined with stereoscope (x7.5). The results are as follows. 1. The difference between 3 RMGICs and a conventional GIC in shear bond strength was not statistically significant. It seemed that RMGICs had lower shear bond strength than resin cement. (p<0.01) 2. The mean scores of marginal leakage had no significant difference between the resin cement and 3 RMGICs but it was much higher in conventional GIC than the RMGICs (p<0.05) 3. It was determined that the manufacturer and the methods of dentin pretreatment determined the pattern of fracture surface and the frequency of adhesive failure between teeth and 3 RMGICs standed as in following order - Vitremer, Advance, Fuji Duet. (p<0.01) When the fracture pattern was analyzed, it could be said that the materials and the method of dentin pretreatment have much effect on bonding states. This means that the dentin bonding agents should be improved. But the limited products in this experiment can not evaluate the physical properties of the entire RMGICs. Therefore a further study which can evaluate various RMGICs should be in progress to develop better cements.